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Beilstein J. Org. Chem. 2013, 9, 26–35, doi:10.3762/bjoc.9.4
Graphical Abstract
Scheme 1: Molecular structures of the investigated four-ring bent-core compounds 1a–1f.
Scheme 2: Synthetic details of the compounds 1a–1f. Reagents and conditions: i. 5% Pd/C, H2, EtOAc stirring, ...
Figure 1: Microphotographs of compounds 1b and 1c in the nematic phase during the cooling cycle. (a) Birefrin...
Figure 2: DSC trace of 1c obtained during initial heating and cooling cycles scanned at a rate of 10 K/min.
Figure 3: Molecular structure of 1a optimized at the DFT level. The bent angle is 143°, and the three dihedra...